Pseudoephedrine AcetateJust a repri

Pseudoephedrine Acetate

Just a reprint. What do I think? Well, I would like the titled material to be analogous to chloroephedrine, but this is just a salt of the amine using acetic as the acid, a result of the isolation process from pills. Much of it is in traffic in Mexico; apparently the superlabs also purchase material which at one time was in pills. The second article is about a seizure.

Meth Synthesis W/ephedrine, HI, Red Phosphorus
by Cousin Singe
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All you people who want an easy meth systhesis – They don’t exist! You have to know some chemistry. Learn some (yes it takes some discipline) or be doomed to fail.

So, again, this information is posted for information purposes only. I accept no responsibility for anyone actually using this. If you do you will be subject to state and federal laws and will be subject to fines and/or imprisonment. If you are stupid enough to actually manufacture meth you WILL probably go to prison. This is the 90's.

So to make meth from ephedrine- Using l- or pseudo ephedrine place 1000 gms of ephedrine, 250gms of red phosphorus, and 1000ml of hydriotic acid in a suitable round bottom flask. Fit the flask with a reflux condenser and reflux the mixture for 48hrs at 120 degrees C. Add a 10% solution of sodium hydroxide until the Ph is 14. You should get an oil layer and a water layer. Separate the oil layer in a separatory funnel and put it a flask with 3 volumes of water. Rig the flask for distillation and distill the oil water mixture until the oil is mostly gone (except for highly colored globs of oil.) In the reciever flask there should be two layers, an upper oil layer and a lower water layer. Separate the oil layer and mix it with 10% hydrochloric acid until the Ph is 7.6. evaporate the water and it will crystallize into methamphetamine hcl.

——

“We have observed that mixtures containing red phosphorus, iodine and either concentrated HCl or glacial acetic acid do convert ephedrine to methamphetamine; however, when the phosphorus is omitted, methamphetamine is not formed. Ephedrine was reacted with red phosphorus and iodine in refluxing water, varying the ratios of red phosphorus and iodine; when red phosphorus and iodine are in excess of ephedrine in a 1:3.8:7.2 molar ratio (ephedrine:red phosphorus:iodine) methamphetamine is formed and the ephedrine is consumed in 8 hours.”

Anyone have any thoughts, experience with the typical E-RP-HA when the usually separate step of creating the hydriotic acid is omitted and the three chemicals are just reacted in refluxing water. It seems like that is what is being described (along with acid substitution).

——

Materials:

1. 30ml bottle tincture iodine containing 2% iodine, sodium iodide 2.4%, alcohol 47%, rest H20

2. 5 Sinustop Herbal Decongestant tablets containing 60mg crystaline pseudoephedrine HCl each mixed with some herbal ingrediants. Or 300mg of ephedrine obtained thru some other method.

3. 5 road flares.

4. Bottle of drain cleaner containg conc. H2SO4

5. Bottle white distilled vinegar

6. Red devil Lye containing sodium hydroxide

7. Spray can of brake cleaner containing 1,1,1 trichloroethylene or 1,1,1 trichloroethane

Procedure:

A. Purifying pseudoephedrine:

1. Take the 5 decongestant capsules, empty their contents into a small funnel with a coffee filter. Pour 50ml of cold water through the filter, and collect the liquid in a small jar.

2. Add a 1/4tsp of lye to the collected liquid. You should immediately smell the odor of ephedrine.

3. Put the resultant solution in another small jar, and add 50ml of brake cleaner, then close the lid and shake vigorously. Let stand so that the layers seperate.

4. Using a turkey baster, suck up the bottom brake cleaner layer out of the jar and put it into a small bowl.

5. Add 50ml of vinegar and heat the resultant mixure over low heat in a frying pan with 1/2 inch of water. Thus a water bath. Do not use a gas stove, since the brake cleaner vapors will produce toxic phosgene if there is contact with a flame. Instead use a hot plate or electric stove at low heat only.

6. Heat the bowl in the water bath until no more liquid is left. At the bottom will be a solid layer of a pseudoephedrine acetate.

B. Preparing the red phosphorus:

1. Scrape the red phosphorus off of the caps of the 5 flares and store for later use. You should get about 0.1g per flare.

C. Preparing the iodine/HI solution:

1. Pour the entire bottle of the iodine tincture into a small ceramic bowl. Heat on the above type water bath until no more alcohol is left. Let cool, put in a small polyethylene jar, and add 0.1ml of the H2SO4 drain cleaner. Thats about 1/4inch of liquid in the end of an eye dropper. This converts the sodium iodide to HI. You now have a solution of iodine and HI. 2. Add the red phosphorus, and heat bottle in a water bath until the purple iodine color goes away.

D. The reaction:

1. Add the pseudoephedrine acetate to the solution of HI/I and phosphorus, and heat on a water bath for 24 hours.

E: Extraction:

1. Cool the reaction solution and add 1/2tsp of lye. Take the solution and perform steps A3-A6. 2. You will end up with methamphetamine acetate that you can scrape from the bowl.

Congradulations! You have circumvented all of law enforcement and have greatly contributed to the end of the “drug war”. (or contributed to the outlaw of all flares, iodine tincture, vignegar, drain cleaners, and auto store chemicals and coffee filters as will happen in the next year)

Best regards, Cousin Singe

————

FAQ fodder…

If methamphetamine looks waxy or oily, it is probably contaminated with the HI salt of meth, an oily by-product of the red-phosphorous/HI reduction of ephedrine–the most prevalent method of clandestine manufacture.

The HI salt is soluble in acetone, while the HCL salt is only very slightly soluble. The HI salt could be washed out, basified, and then precipitated with HCl gas to give methamphetmine HCL.

When completely dry, methamphetamine HCL is soluble in chloroform, while ephedrine HCL is not. This would provide a convenient method of separation.

[Reference: Skinner, Harry F., "Methamphetamine Synthesis Via Hydriotic Acid/Red Phosphorous Reduction Of Ephedrine," Forensic Science International, Vol 48, 1990, pp. 123-134]

Kết quả (Pháp) 1:

Acétate de pseudoéphédrineJuste une réimpression. Ce que je pense ? Eh bien, je voudrais le matériel pour être analogue: '' il a chloroephedrine, mais c'est juste un sel de l'amine en utilisant l'acide acétique et comme le résultat du processus d'isolement des pilules. Une grande partie de celui-ci est en circulation au Mexique ; apparemment les superlaboratoires également achètent matériel qui a été à un moment donné en pilules. Le second article est au sujet et les saisies abusives.Meth synthèse W/éphédrine, HI, rouge phosphoreCousin doubleraitAVIS : Tous concernés certains fichiers texte et les messages contenus sur ce site traitent des activités et dispositifs qui seraient dans "de divers fédéral, État et lois locales si réellement effectués ou construit. Les webmasters de ce site ne préconisent pas la rupture de toute règle de droit. Nos fichiers texte et les bases de messages sont à titre informatif seulement. Nous vous recommandons de contacter vos autorités policières locales avant d'entreprendre tout projet fondée sur des renseignements obtenus de cet appareil ou de tout autre site web. Nous ne garantissons pas que les informations contenues sur ce système est correcte, viable ou factuel. Nous ne sommes pas responsables, nous déclinons toute responsabilité pour les dommages résultant de l'utilisation de toute information sur ce site.Tout ce que vous les gens qui veulent une syntèse de meth facile – ils n'existent pas ! Il faut savoir quelques chimie. Apprendre à certains (oui il faut une discipline) ou être vouées à l'échec.Donc, encore une fois, cette information est affichée uniquement à des fins d'information. J'ai n'accepter aucune responsabilité pour toute personne qui utilise en fait cela. Si vous ne vous sera soumis à l'État et les lois fédérales et feront l'objet d'amendes ou d'emprisonnement. Si vous êtes stupide assez qui fabriquent réellement meth que vous irez probablement à la prison. Il s'agit de la 90 ' s.Donc faire meth d'éphédrine-utiliser l- ou pseudo éphédrine placer 1000 gms d'éphédrine, 250gms du phosphore rouge et 1000 ml d'acide hydriotic dans un ballon à fond rond approprié. Monter le ballon avec un réfrigérant à reflux et reflux le mélange pendant 48 h à 120 degrés C. Ajouter 10 % solution d'hydroxyde de sodium jusqu'à ce que le Ph soit 14. Vous devriez obtenir une couche d'huile et de la couche d'eau. Séparez la couche d'huile dans une ampoule à décanter et mettre et le ballon avec 3 volumes d'eau. Gréer le ballon de distillation et de distiller le mélange de l'eau d'huile jusqu'à ce que l'huile est pour la plupart disparu (à l'exception des globules fortement colorés de l'huile.) Dans le récepteur fiole il devrait être de deux couches : une couche d'huile supérieure et la couche d'eau et en réduire. Séparer la couche d'huile et mélanger avec l'acide chlorhydrique à 10 % jusqu'à ce que le Ph soit 5.0. faire évaporer l'eau et il va se cristalliser en chlorhydrate de méthamphétamine.——“We have observed that mixtures containing red phosphorus, iodine and either concentrated HCl or glacial acetic acid do convert ephedrine to methamphetamine; however, when the phosphorus is omitted, methamphetamine is not formed. Ephedrine was reacted with red phosphorus and iodine in refluxing water, varying the ratios of red phosphorus and iodine; when red phosphorus and iodine are in excess of ephedrine in a 1:3.8:7.2 molar ratio (ephedrine:red phosphorus:iodine) methamphetamine is formed and the ephedrine is consumed in 8 hours.”Anyone have any thoughts, experience with the typical E-RP-HA when the usually separate step of creating the hydriotic acid is omitted and the three chemicals are just reacted in refluxing water. It seems like that is what is being described (along with acid substitution).——Materials:1. 30ml bottle tincture iodine containing 2% iodine, sodium iodide 2.4%, alcohol 47%, rest H202. 5 Sinustop Herbal Decongestant tablets containing 60mg crystaline pseudoephedrine HCl each mixed with some herbal ingrediants. Or 300mg of ephedrine obtained thru some other method.3. 5 road flares.4. Bottle of drain cleaner containg conc. H2SO45. Bottle white distilled vinegar6. Red devil Lye containing sodium hydroxide7. Spray can of brake cleaner containing 1,1,1 trichloroethylene or 1,1,1 trichloroethaneProcedure:A. Purifying pseudoephedrine:1. Take the 5 decongestant capsules, empty their contents into a small funnel with a coffee filter. Pour 50ml of cold water through the filter, and collect the liquid in a small jar.2. Add a 1/4tsp of lye to the collected liquid. You should immediately smell the odor of ephedrine.3. Put the resultant solution in another small jar, and add 50ml of brake cleaner, then close the lid and shake vigorously. Let stand so that the layers seperate.4. Using a turkey baster, suck up the bottom brake cleaner layer out of the jar and put it into a small bowl.5. Add 50ml of vinegar and heat the resultant mixure over low heat in a frying pan with 1/2 inch of water. Thus a water bath. Do not use a gas stove, since the brake cleaner vapors will produce toxic phosgene if there is contact with a flame. Instead use a hot plate or electric stove at low heat only.6. Heat the bowl in the water bath until no more liquid is left. At the bottom will be a solid layer of a pseudoephedrine acetate.B. Preparing the red phosphorus:1. Scrape the red phosphorus off of the caps of the 5 flares and store for later use. You should get about 0.1g per flare.C. Preparing the iodine/HI solution:1. Pour the entire bottle of the iodine tincture into a small ceramic bowl. Heat on the above type water bath until no more alcohol is left. Let cool, put in a small polyethylene jar, and add 0.1ml of the H2SO4 drain cleaner. Thats about 1/4inch of liquid in the end of an eye dropper. This converts the sodium iodide to HI. You now have a solution of iodine and HI. 2. Add the red phosphorus, and heat bottle in a water bath until the purple iodine color goes away.D. The reaction:1. Add the pseudoephedrine acetate to the solution of HI/I and phosphorus, and heat on a water bath for 24 hours.E: Extraction:1. Cool the reaction solution and add 1/2tsp of lye. Take the solution and perform steps A3-A6. 2. You will end up with methamphetamine acetate that you can scrape from the bowl.Congradulations! You have circumvented all of law enforcement and have greatly contributed to the end of the “drug war”. (or contributed to the outlaw of all flares, iodine tincture, vignegar, drain cleaners, and auto store chemicals and coffee filters as will happen in the next year)Best regards, Cousin Singe————FAQ fodder…If methamphetamine looks waxy or oily, it is probably contaminated with the HI salt of meth, an oily by-product of the red-phosphorous/HI reduction of ephedrine–the most prevalent method of clandestine manufacture.The HI salt is soluble in acetone, while the HCL salt is only very slightly soluble. The HI salt could be washed out, basified, and then precipitated with HCl gas to give methamphetmine HCL.When completely dry, methamphetamine HCL is soluble in chloroform, while ephedrine HCL is not. This would provide a convenient method of separation.[Reference: Skinner, Harry F., "Methamphetamine Synthesis Via Hydriotic Acid/Red Phosphorous Reduction Of Ephedrine," Forensic Science International, Vol 48, 1990, pp. 123-134]